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Solid State NMR and tools for molecules, materials and biological systems

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Educational program: Advanced Spectroscopic and Analytical Techniques

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Academic year 2025/2026

Teachers
Roberto Gobetto (Lecturer)
Michele R. Chierotti (Lecturer)
Angelo Gallo (Lecturer)
Teaching period
Second semester
Type
Basic
Credits/Recognition
4 CFU
Course disciplinary sector (SSD)
SSD: CHIM/03 - general and inorganic chemistry
Delivery
Formal authority
Language
English
Attendance
Obligatory
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Sommario del corso

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Program

- Introduction to Solid-State NMR

  • NMR interaction tensors
  • Dipolar interaction
  • Chemical shielding
  • Relaxation times

- From low to high resolution spectra

  • HPPD and MAS
  • Cross polarization

- High resolution Solid-State NMR of 1H and 19F

- High resolution Solid-State NMR of Quadrupolar Nuclei

- Application of Solid-State NMR:

  • Organic Molecules
  • Polymorphic forms
  • Polymers
  • Materials: Zeolites and Inorganic Compounds

- High resolution Solid-State NMR of proteins

  • From low to ultrafast spinning
  • Experiments for assignment and structure calculations
  • Protein dynamics

Suggested readings and bibliography

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Class scheduleV

Lessons: from 09/02/2026 to 24/02/2026

Notes:
Lessons all in February

- Feb 9: 9-12 (3h) - Aula Diagonale (Prof Gobetto)
- Feb 11: 9-12 (3h) - Aula Disegno (Prof Gobetto)
- Feb 13: 9-12 (3h) - Aula Diagonale (Prof Chierotti)
- Feb 18: 9-12 (3h) - Aula D1 (Prof Chierotti)
- Feb 24: 9-13 (4h) - Aula Diagonale (Dr Gallo)

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