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Solid State NMR and tools for molecules, materials and biological systems

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Advanced Spectroscopic and Analytical Techniques

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Academic year 2023/2024

Teachers
Roberto Gobetto (Lecturer)
Michele R. Chierotti (Lecturer)
Angelo Gallo (Lecturer)
Teaching period
Second semester
Type
Basic
Credits/Recognition
4 CFU
Course disciplinary sector (SSD)
CHIM/03 - general and inorganic chemistry
Delivery
Formal authority
Language
English
Attendance
Obligatory
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Sommario del corso

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Program

- Introduction to Solid-State NMR

  • NMR interaction tensors
  • Dipolar interaction
  • Chemical shielding
  • Relaxation times

- From low to high resolution spectra

  • HPPD and MAS
  • Cross polarization

- High resolution Solid-State NMR of 1H and 19F

- High resolution Solid-State NMR of Quadrupolar Nuclei

- Application of Solid-State NMR:

  • Organic Molecules
  • Polymorphic forms
  • Polymers
  • Materials: Zeolites and Inorganic Compounds

- High resolution Solid-State NMR of proteins

  • From low to ultrafast spinning
  • Experiments for assignment and structure calculations
  • Protein dynamics

Suggested readings and bibliography

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Class scheduleV

Lessons: from 07/02/2024 to 23/02/2024

Notes: Dates, time and place of the lessons and of the exam:

Feb 7: 14-17 (3h) (AULA D1)
Feb 8: 14-17 (3h) (AULA D1)
Feb 14: 14-17 (3h) (AULA D1)
Feb 16: 14-17 (3h) (AULA D1)
Feb 23: 14-18 (4h) (AULA D1)

The lessons can also be followed by connecting to the following virtual rooms:
7th February 2022 - 2pm - 5pm – R. Gobetto: https://unito.webex.com/meet/roberto.gobetto

8th February 2022 - 2pm - 5pm - R. Gobetto: https://unito.webex.com/meet/roberto.gobetto

14th February 2022 - 2pm - 5pm – M.R. Chierotti: https://unito.webex.com/meet/michele.chierotti

14th February 2022 - 2pm - 5pm – M.R. Chierotti: https://unito.webex.com/meet/michele.chierotti

23th February 2022 - 2pm - 5pm – A. Gallo: https://unito.webex.com/meet/angelo.gallo

23th February 2022 - 5pm - 6pm – Test: the test can only be done in person except for those on assignment abroad (https://unito.webex.com/meet/angelo.gallo).

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