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Solid State NMR and tools for molecules, materials and biological systems
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Advanced Spectroscopic and Analytical Techniques
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Academic year 2021/2022
- Teaching staff
- Prof. Roberto Gobetto (Titolare del corso)
Prof. Michele R. Chierotti (Titolare del corso)
Dott. Angelo Gallo (Titolare del corso) - Teaching period
- Second semester
- Type
- Basic
- Credits/Recognition
- 4 CFU
- Course disciplinary sector (SSD)
- CHIM/03 - general and inorganic chemistry
- Delivery
- Formal authority
- Language
- English
- Attendance
- Obligatory
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Sommario del corso
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Program
- Introduction to Solid-State NMR
- NMR interaction tensors
- Dipolar interaction
- Chemical shielding
- Relaxation times
- From low to high resolution spectra
- HPPD and MAS
- Cross polarization
- High resolution Solid-State NMR of 1H and 19F
- High resolution Solid-State NMR of Quadrupolar Nuclei
- Application of Solid-State NMR:
- Organic Molecules
- Polymorphic forms
- Polymers
- Materials: Zeolites and Inorganic Compounds
- High resolution Solid-State NMR of proteins
- From low to ultrafast spinning
- Experiments for assignment and structure calculations
- Protein dynamics
Suggested readings and bibliography
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Note
Dates, time and place of the lessons:
June 29: 14-17 (3h) (AULA AVOGADRO)June 30: 14-17 (3h) (AULA DISEGNO)July 1: 14-17 (3h) (AULA DIAGONALE)July 4: 14-17 (3h) (AULA DISEGNO)July 5: 14-18 (4h) (AULA DISEGNO)- Oggetto:
